Carbon-13 NMR Spectral Problems

Name: Carbon-13 NMR Spectral Problems
Brand: Humana Press Inc.
SKU: 9780896030107
Price: 824.66 RON
Availability: InStock

Autor: Robert B. Bates, William A. Beavers

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Legare: Copertă tare

Editura: Humana Press Inc.

Disponibilitate: În depozitul extern

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With the advent of Fourier transform spectrometers of great sensitivity, it has become practical to...

Informații despre carte

Autor

Robert B. Bates, William A. Beavers

Limbă

engleză

Legare

Carte - Copertă tare

Pagini

259

EAN

9780896030107

ISBN

0896030105

Enbook ID

01400486

Editura

Humana Press Inc.

Greutate

682

Dimensiuni

203 x 203 x 20

Descriere completă

With the advent of Fourier transform spectrometers of great sensitivity, it has become practical to obtain carbon-13 nuclear magnetic resonance (C-13 NMR; l3C NMR; CMR) spectra routinely on organic molecules, and this technique has become one of the highest utility in determining structures of organic unknowns. When the usual spectrometric techniques proton magnetic resonance (H-I NMR; IH NMR; PMR), infrared (lR), mass (MS), and ultraviolet (UV)-do not readily reveal a compound's structure, a C-13 NMR spectrum will often provide sufficient additional information to yield it unequivocally. With this in mind, the present work was designed to give advanced undergraduates, graduate students, and practicing chemists a working knowledge of and facility with the use of this valuable technique. Some familiarity with other spectrometric techniques is assumed (recommended book: Silverstein, Bassler, and Morrill, Spectrometric Identification of Organic Compounds), but no prior knowledge of C-13 NMR -which is treated very lightly, if at all, in the widely used elementary organic texts-is necessary. A discussion of C-13 NMR spectroscopy is followed by 125 problems, each consisting of a molecular formula, two types of C-13 NMR spectra (partially and completely proton decoupled, with connecting lines to facilitate multiplicity assignments), an integrated H-I NMR spectrum, and the most important IR, UV, and MS data. These problems have been very carefully prepared, thoroughly tested by students at the University of Arizona, and we believe that very few errors remain.

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